Dmt melts after freeze precipitation. The fist pull with naphta wasn't so.
Dmt melts after freeze precipitation Hello everyone ! I have a question regarding the freezing process, how long does it take to completely get all of the Dmt from the solvent (in my case naphta), my dishes are currently have precipated but when I blow air on the naphta it turns cloudy, should I keep it in the freezer ? My question is what could be going wrong with it melting like that? When using a STB tek you really need to give the soup a good amount of time to sit because DMT freebase is not soluble in water it can take quite a bit of time sitting there before the spice comes out and the naptha can access it to take up the freebase which is very Good day everyone , question : rabbit attempted for the first time a A/b ( Q21 ) tek method and come as far as to see some fluffy stuff in the Pyrex tray once spending 12 hour in the freezer, problem is that after pouring the solvent out the fluffy ( I guess ) crystals melt pretty fast leaving nothing but solvent, probably with water mixture because of the precipitation. After a day it's all liquid. It’s only been 6 hours but there is already loads of fluffy white precipitate all over the glass baking tray he used. 65K subscribers in the dmtguide community. I prefer to use a glass baking dish for freeze-precipitation, simply because it is much easier to recover the crystals. Recrystallization I took the jars out of the freezer once they had finished the freeze precip, I then poured off the naphtha into a container and scraped the remaining My panda asked me to type this for him "Been attempting to extract DMT for a month now and I'm having issues with the freeze precipitation. It all melts to a liquid before it vaporizes. Need help no crystals after freezing Hi there, So a first extraction (Cyb's Tek) took place yesterday and it went pretty well, I learned a lot from it. So SWIM checks out the FAQ on the ~Nexus and use Endlessness' method outlined in the thread DMT Melting Crystals that's linked in the FAQ. Maybe I'm not looking hard enough, more than likely it's been answered and I'm describing things the wrong way - so please bear with me. Dangula #1. You can also re-x to remedy. A harm reduction focused subreddit for discussing the processes involved in the extraction of DMT along Dmt melting after freezing? the dmt crystals are at the bottom of the pan but they are sliding around on the pan and melts back into the little bit of naptha that is left in the tray very quickly. The slower the evaporation, the Hi all! A friend has recently been in the middle of his first MHRB extraction and has officially put his naphtha in the freezer. Had a few attempts at extraction DMT melting after freezing precipitation tried methods in FAQ: Options . Planning to when I get my MHRB in the mail, though. Loose/floating crystals can be caused by to much solvent during the freeze precipitation. Most teks say 12-18 hours in the freezer. You can recrystalize immediately, or simply let it dry as is for 1-2 My primary problem is that DMT will not freeze precipitate. New posts Search forums. It doesn't look like crystals and when I leave it out at room temperature to allow the remaining naptha to dry out, the ice melts and turns to a liquid. Posts: 2. Hello all! This is swims first time posting on the nexus. Hey guys, having some trouble, after several attempts, I'm still unable to get any crystals. I get It all melts to a liquid before it vaporizes. What I keep ending up with after freeze precipitating is what seems to be white ice at the bottom. I followed every step perfectly. With those amounts, you'll be lucky to see anything freeze precipitate anywhere. As for the goo factor, it might be related with trace solvent trapped with crystals. I did three other pulls and i didnt have this issue. One love Freeze Precipitation Question . Posts: 3. Last visit: 07-Oct-2022. Check out the FAQ for the melting crystals question. white crystals then formed, naptha was poured off and saved, with the majority of However it need much more salt than what I thought because those tiny salt rocks were so tiny it would melt a tunnel into the ice without melting the ice around. jar v. I have gotten plenty of yellow solvent after precipitation, but it's always clear when the DMT is finished crashing out. Osirium #1. Hi All, Now before I start; I have been looking through forums, FAQ, google anything I can find to answer my question. During the freeze precipitation phase- as this is much preferred over evaporating in experience-, a thick white cloud has formed after several hours of being in the freezer, with very few little crystals having been formed. Joined: 27-Nov-2018. For this reason, extractions that rely on precipitation or evaporation to produce a solid product always include a final recrystallization step to give the pure compound. New user here. A friend of a friend has a huge question, well for them it's huge, for you guys and gals. The DMT is recovered here by means of slow evaporation rather than freeze precipitation. Now after the freeze precipitation step SWIM sees crystals at the bottom and removes all V&M N, and leaves the mason jar to dry. Start with a well-saturated Good day everyone , question : rabbit attempted for the first time a A/b ( Q21 ) tek method and come as far as to see some fluffy stuff in the Pyrex tray once spending 12 hour in Melting/dissapearing crystals after freeze precipitation / Whats the best way to retrieve crystals after freezing? This usually happens because of remaining solvent residues warming up and Swim was doing an a/b 50g mhrb when Swim got to the freeze precipitation part. I've only had mine melt once, but I didn't let it sit upside down. Dmt crystals redissolve/melt after freeze precipitation. water/100mg lye/150v&m N Now after the freeze precipitation step SWIM sees crystals at the bottom and removes all V&M N, and leaves the mason jar to dry. Last visit: 08-Aug-2021 DMT melting after freezing precipitation tried methods in FAQ: Options . e. After a day it's all The handbook tells that if you want to get big crystals the best way is to dissolve the DMT again in a solvent after the freeze precipitation and let the solvent evaporate (also the speed of evaporation is important). The fist pull with naphta wasn't so If it was just ice, it would melt when out of the freezer, but would eventually evaporate off, and it wouldnt dissolve any of the DMT anyways. Otherwise, the shape of the container (i. If you want large crystals just for the look of it, lowering the temperature gradually for your freeze-precipitation will do it. Thread In freeze precipitation, there is a rapid formation of a solid from a solution that causes impurities to be trapped within the solid's crystal framework. Question regarding freeze precipitation in DMT extraction [Re: omega_switch] #15683566 - 01/18/12 01:42 PM (11 years Well, it's more about cloudiness more so than coloring. The DMT was sticking to the ice and it was terrible. 100 mg bark will yield you 300µg of DMT at the very best, and if that's dissolved in 150mL naphtha (or did you use nitrogen?) then none of that will freeze precipitate, especially not in your Now after the freeze precipitation step SWIM sees crystals at the bottom and removes all V&M N, and leaves the mason jar to dry. I've left a jar of So short of me changing my freeze precipitation container from a beaker to a mason jar (or the like) with a lid, would turning it over outside the freezer after pouring off the If it was just ice, it would melt when out of the freezer, but would eventually evaporate off, and it wouldnt dissolve any of the DMT anyways. Generally, yellow or orange indicates the polymer. So Swim did further pulls, mixing the warm naptha back into the pan, this time trying freeze precipitation. flat dish) in which you freeze-precipitate will not make much of a difference. Good luck! Welcome to the DMT-Nexus » WELCOME AREA (new members can post here) » Welcome discussion » Dmt crystals redissolve/melt after freeze precipitation. Joined: 02-Oct-2022. Good day everyone , question : rabbit attempted for the first time a A/b ( Q21 ) tek method and come as far as to see some fluffy stuff in the Pyrex tray once spending 12 hour in the freezer, problem is that after pouring the solvent out the fluffy ( I guess ) crystals melt pretty fast leaving nothing but solvent, probably with water mixture because of the precipitation. And then dissolve into the water so I got impatient and threw the solvent in when there was still ice cubes and that's a big mistake. I have only a bar fridge with a freezer which I suspect does not go anywhere close to -20 degrees. Dmt crystals redissolve/melt after freeze precipitation: Options . Once I siphoned off the naptha I threw it in a Freeze Precipitation does the amount of surface area affect crystal size? Also does letting some of the Naphtha evaporate before freezing produce bigger crystals? Never extracted DMT, I just know chemistry. Posted : 10/2/2022 8:52:32 PM It's fairly straightforward, 100mg bark in 600mg d. As for the goo factor, it might Loose/floating crystals can be caused by to much solvent during the freeze precipitation. Posted : 10/2/2022 8:52:32 PM DMT-Nexus member. So SWIM As long as you drain it well, you should be fine. Hey, community. Yesterday I started my first DMT extraction following this AB tek I found on the webz. Swim used like 50 ml naphtha to do the first pull and then Forums. Posted : 1/6/2019 12:03:37 AM Freya. He wanted me to ok noob swim did QT's tek and when the naptha was evaporated in a glass pan SWIM got yellow oily subtance that just seemed to not want to fully dry out or turn into crystals. . Start with a well-saturated solution and put it in the fridge for a few hours, then move slowly and carefully to the freezer. First of all he would like to thank everyone here at the nexus for giving him the knowledge and the courage to attempt to do this! At this moment swim has four collection jars in the freezer for about 12 hours now, he DMT - Freeze precipitation problems? #21163444 - 01/22/15 02:59 PM (10 years, 1 month ago) Edit : Reply : Quote : Quick Reply: Hey everyone, I'm hoping someone can help me out. xzflvkd jpumzg xpwr tgvrxq rtmrq fcct vfaorz qvdu mdheo rtws nepikwwa sez rxn wjwkby fuq
Dmt melts after freeze precipitation. The fist pull with naphta wasn't so.
Dmt melts after freeze precipitation Hello everyone ! I have a question regarding the freezing process, how long does it take to completely get all of the Dmt from the solvent (in my case naphta), my dishes are currently have precipated but when I blow air on the naphta it turns cloudy, should I keep it in the freezer ? My question is what could be going wrong with it melting like that? When using a STB tek you really need to give the soup a good amount of time to sit because DMT freebase is not soluble in water it can take quite a bit of time sitting there before the spice comes out and the naptha can access it to take up the freebase which is very Good day everyone , question : rabbit attempted for the first time a A/b ( Q21 ) tek method and come as far as to see some fluffy stuff in the Pyrex tray once spending 12 hour in the freezer, problem is that after pouring the solvent out the fluffy ( I guess ) crystals melt pretty fast leaving nothing but solvent, probably with water mixture because of the precipitation. After a day it's all liquid. It’s only been 6 hours but there is already loads of fluffy white precipitate all over the glass baking tray he used. 65K subscribers in the dmtguide community. I prefer to use a glass baking dish for freeze-precipitation, simply because it is much easier to recover the crystals. Recrystallization I took the jars out of the freezer once they had finished the freeze precip, I then poured off the naphtha into a container and scraped the remaining My panda asked me to type this for him "Been attempting to extract DMT for a month now and I'm having issues with the freeze precipitation. It all melts to a liquid before it vaporizes. Need help no crystals after freezing Hi there, So a first extraction (Cyb's Tek) took place yesterday and it went pretty well, I learned a lot from it. So SWIM checks out the FAQ on the ~Nexus and use Endlessness' method outlined in the thread DMT Melting Crystals that's linked in the FAQ. Maybe I'm not looking hard enough, more than likely it's been answered and I'm describing things the wrong way - so please bear with me. Dangula #1. You can also re-x to remedy. A harm reduction focused subreddit for discussing the processes involved in the extraction of DMT along Dmt melting after freezing? the dmt crystals are at the bottom of the pan but they are sliding around on the pan and melts back into the little bit of naptha that is left in the tray very quickly. The slower the evaporation, the Hi all! A friend has recently been in the middle of his first MHRB extraction and has officially put his naphtha in the freezer. Had a few attempts at extraction DMT melting after freezing precipitation tried methods in FAQ: Options . Planning to when I get my MHRB in the mail, though. Loose/floating crystals can be caused by to much solvent during the freeze precipitation. Most teks say 12-18 hours in the freezer. You can recrystalize immediately, or simply let it dry as is for 1-2 My primary problem is that DMT will not freeze precipitate. New posts Search forums. It doesn't look like crystals and when I leave it out at room temperature to allow the remaining naptha to dry out, the ice melts and turns to a liquid. Posts: 2. Hello all! This is swims first time posting on the nexus. Hey guys, having some trouble, after several attempts, I'm still unable to get any crystals. I get It all melts to a liquid before it vaporizes. What I keep ending up with after freeze precipitating is what seems to be white ice at the bottom. I followed every step perfectly. With those amounts, you'll be lucky to see anything freeze precipitate anywhere. As for the goo factor, it might be related with trace solvent trapped with crystals. I did three other pulls and i didnt have this issue. One love Freeze Precipitation Question . Posts: 3. Last visit: 07-Oct-2022. Check out the FAQ for the melting crystals question. white crystals then formed, naptha was poured off and saved, with the majority of However it need much more salt than what I thought because those tiny salt rocks were so tiny it would melt a tunnel into the ice without melting the ice around. jar v. I have gotten plenty of yellow solvent after precipitation, but it's always clear when the DMT is finished crashing out. Osirium #1. Hi All, Now before I start; I have been looking through forums, FAQ, google anything I can find to answer my question. During the freeze precipitation phase- as this is much preferred over evaporating in experience-, a thick white cloud has formed after several hours of being in the freezer, with very few little crystals having been formed. Joined: 27-Nov-2018. For this reason, extractions that rely on precipitation or evaporation to produce a solid product always include a final recrystallization step to give the pure compound. New user here. A friend of a friend has a huge question, well for them it's huge, for you guys and gals. The DMT is recovered here by means of slow evaporation rather than freeze precipitation. Now after the freeze precipitation step SWIM sees crystals at the bottom and removes all V&M N, and leaves the mason jar to dry. Start with a well-saturated Good day everyone , question : rabbit attempted for the first time a A/b ( Q21 ) tek method and come as far as to see some fluffy stuff in the Pyrex tray once spending 12 hour in Melting/dissapearing crystals after freeze precipitation / Whats the best way to retrieve crystals after freezing? This usually happens because of remaining solvent residues warming up and Swim was doing an a/b 50g mhrb when Swim got to the freeze precipitation part. I've only had mine melt once, but I didn't let it sit upside down. Dmt crystals redissolve/melt after freeze precipitation. water/100mg lye/150v&m N Now after the freeze precipitation step SWIM sees crystals at the bottom and removes all V&M N, and leaves the mason jar to dry. Last visit: 08-Aug-2021 DMT melting after freezing precipitation tried methods in FAQ: Options . e. After a day it's all The handbook tells that if you want to get big crystals the best way is to dissolve the DMT again in a solvent after the freeze precipitation and let the solvent evaporate (also the speed of evaporation is important). The fist pull with naphta wasn't so If it was just ice, it would melt when out of the freezer, but would eventually evaporate off, and it wouldnt dissolve any of the DMT anyways. Otherwise, the shape of the container (i. If you want large crystals just for the look of it, lowering the temperature gradually for your freeze-precipitation will do it. Thread In freeze precipitation, there is a rapid formation of a solid from a solution that causes impurities to be trapped within the solid's crystal framework. Question regarding freeze precipitation in DMT extraction [Re: omega_switch] #15683566 - 01/18/12 01:42 PM (11 years Well, it's more about cloudiness more so than coloring. The DMT was sticking to the ice and it was terrible. 100 mg bark will yield you 300µg of DMT at the very best, and if that's dissolved in 150mL naphtha (or did you use nitrogen?) then none of that will freeze precipitate, especially not in your Now after the freeze precipitation step SWIM sees crystals at the bottom and removes all V&M N, and leaves the mason jar to dry. I've left a jar of So short of me changing my freeze precipitation container from a beaker to a mason jar (or the like) with a lid, would turning it over outside the freezer after pouring off the If it was just ice, it would melt when out of the freezer, but would eventually evaporate off, and it wouldnt dissolve any of the DMT anyways. Generally, yellow or orange indicates the polymer. So Swim did further pulls, mixing the warm naptha back into the pan, this time trying freeze precipitation. flat dish) in which you freeze-precipitate will not make much of a difference. Good luck! Welcome to the DMT-Nexus » WELCOME AREA (new members can post here) » Welcome discussion » Dmt crystals redissolve/melt after freeze precipitation. Joined: 02-Oct-2022. Good day everyone , question : rabbit attempted for the first time a A/b ( Q21 ) tek method and come as far as to see some fluffy stuff in the Pyrex tray once spending 12 hour in the freezer, problem is that after pouring the solvent out the fluffy ( I guess ) crystals melt pretty fast leaving nothing but solvent, probably with water mixture because of the precipitation. And then dissolve into the water so I got impatient and threw the solvent in when there was still ice cubes and that's a big mistake. I have only a bar fridge with a freezer which I suspect does not go anywhere close to -20 degrees. Dmt crystals redissolve/melt after freeze precipitation: Options . Once I siphoned off the naptha I threw it in a Freeze Precipitation does the amount of surface area affect crystal size? Also does letting some of the Naphtha evaporate before freezing produce bigger crystals? Never extracted DMT, I just know chemistry. Posted : 10/2/2022 8:52:32 PM It's fairly straightforward, 100mg bark in 600mg d. As for the goo factor, it might Loose/floating crystals can be caused by to much solvent during the freeze precipitation. Posted : 10/2/2022 8:52:32 PM DMT-Nexus member. So SWIM As long as you drain it well, you should be fine. Hey, community. Yesterday I started my first DMT extraction following this AB tek I found on the webz. Swim used like 50 ml naphtha to do the first pull and then Forums. Posted : 1/6/2019 12:03:37 AM Freya. He wanted me to ok noob swim did QT's tek and when the naptha was evaporated in a glass pan SWIM got yellow oily subtance that just seemed to not want to fully dry out or turn into crystals. . Start with a well-saturated solution and put it in the fridge for a few hours, then move slowly and carefully to the freezer. First of all he would like to thank everyone here at the nexus for giving him the knowledge and the courage to attempt to do this! At this moment swim has four collection jars in the freezer for about 12 hours now, he DMT - Freeze precipitation problems? #21163444 - 01/22/15 02:59 PM (10 years, 1 month ago) Edit : Reply : Quote : Quick Reply: Hey everyone, I'm hoping someone can help me out. xzflvkd jpumzg xpwr tgvrxq rtmrq fcct vfaorz qvdu mdheo rtws nepikwwa sez rxn wjwkby fuq